1000 mesh graphite equals approx 13 μm particle size, widely used in lithium battery anode materials, high-conductive slurry, thermal interface materials, high-end anti-corrosion coatings and aerospace composite materials. To stably produce qualified 1000 mesh fine graphite, adopt low-temperature ultrafine grinding + high-precision airflow classification process, strictly control particle size distribution, retain complete graphite flake structure, minimize iron contamination and low ash content.
1. High-Grade Raw Material Standard
- Raw material: High crystalline natural flake graphite / high purity artificial graphite
- Fixed carbon content: ≥98%
- Ash content: ≤1.0%
- Iron content: ≤80 ppm
- Raw material moisture: ≤0.5%
- Remove gangue, silt and hard abrasive impurities completely in advance
2. Complete Production Process
Step 1 Pre-treatment & Purification
- Sort out large impurities manually
- Water washing to remove surface mud and fine soil
- Low temperature drying at 60–75°C, final moisture controlled below 0.4%
- Primary coarse crushing to 3–8 mm uniform particles
Step 2 Core Ultrafine Grinding (Key Process)
Select dedicated ultrafine grinding equipment, ordinary Raymond mill cannot reach stable 1000 mesh:
- Airflow Jet Mill (Best for high-end advanced grade)No mechanical contact grinding, ultra-low iron pollution, complete flake retention, ideal for battery and electronic grade graphite
- Vertical Ultrafine Grinding Mill (Mass production preferred)Large output, stable fineness, suitable for industrial large-scale 1000 mesh graphite
- Ring Roller Ultrafine MillCost-effective, stable fineness for general advanced coating grade
Grinding core rule: Keep grinding temperature below 65°C to avoid graphite oxidation and crystal structure damage.
Step 3 High-Precision Air Classification (Decisive for 1000 Mesh)
- Match high-speed dynamic classifier, adjust rotor speed to fix cutting particle size at 13 μm
- All particles larger than 13 μm return to grinding chamber for re-grinding
- Control finished product index: 1000 mesh passing rate ≥98%, D97 ≤15 μm
- Stabilize air volume and wind pressure to avoid fineness fluctuation
Step 4 Multi-stage Iron Removal & Deep Purification
- Install high-strength magnetic separator (12000–15000 Gauss) to remove mechanical iron impurities
- For battery-grade advanced graphite: add acid washing process to reduce ash and harmful metal elements
- Remove micro abrasive impurities to ensure high stability in high-end formulas
Step 5 De-agglomeration & Dispersion Treatment
Add trace non-toxic grinding dispersant during production to eliminate powder agglomeration, greatly improve dispersion performance in resin, solvent and slurry system.
Step 6 Homogenization & Finished Collection
- Uniform mixing of finished fine graphite powder
- Pulse dust collection full recovery, no waste loss
- Sealed moisture-proof packaging
3. Core Technical Control Points
- Do not pursue excessive fineness blindly, protect graphite flake integrity to maintain excellent conductivity and thermal conductivity
- Keep feeding speed stable, avoid sudden fast feeding causing coarse powder overflow
- Regularly check and replace classifier blades to ensure consistent classification effect
- Strictly isolate external moisture, prevent fine graphite powder from absorbing moisture and caking
- Adjust classifier speed slightly according to raw material hardness to lock 1000 mesh stably
4. Quality Index for Advanced 1000 Mesh Graphite
- Fineness: 1000 mesh pass rate ≥98%
- Median particle size D50: 11–13 μm
- Moisture: ≤0.4%
- Ash content: ≤1.0%
- Iron content: ≤80 ppm
- Good fluidity, no hard agglomeration
- Excellent dispersion in oil phase and water phase systems
5. Common Production Troubleshooting
- Fineness not fine enough
Reason: Low classifier speed, insufficient grinding time
- Solution: Increase classification rotor speed, reduce unit feeding volume
- Serious powder agglomeration
Reason: High moisture, excessive fine powder
- Solution: Strengthen drying, optimize airflow balance
- High iron impurity content
Reason: Grinding liner and roller wear seriously
- Solution: Replace wear-resistant ceramic accessories, enhance multi-stage iron removal
- Unstable batch fineness
Reason: Unstable raw material hardness and uneven feeding
- Solution: Pre-blend raw materials, adopt automatic constant feeding system
6. Matching Advanced Application Directions
- Lithium ion battery anode auxiliary material
- High thermal conductivity silicone grease & thermal conductive filler
- Electronic conductive silver paste / carbon conductive slurry
- High temperature resistant high-grade industrial coatings
- Carbon fiber composite reinforcing filler
- EMI electromagnetic shielding materials